Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Bromopyruvic Acid | HCID 70684 | — |
| Reactant | N-(4-Chloro-3-methoxyphenyl)thiourea | HCID 86056613 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86056614 | HCID 86056614 | — |
Reaction Steps
A mixture of 7.8 g (36 mmol) 1-(4-chloro-3-methoxyphenyl)-thiourea, and 6.2 g (36 mmol) bromopyruvic acid in 80 ml ethanol was heated to 60° C. for 1 h. The precipitate was filtered off and washed with small portions of cold ethanol to yield after drying 10.0 g (98%) of the title compound as crystalline solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07371751B2 |
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| Source dataset | uspto-grants-2008_05 |
|---|
| ORD ID | ord-320ea0b15fcc427e9786dbe04d53929f |
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| Source note | uspto-grants-2008_05 |
|---|
