HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 4-[(Z)-2-cyano-2-(3,4-dimethoxy-phenyl)-vinyl]-phenyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | (Z)-2-(3,4-dimethoxyphenyl)-3-(4-hydroxyphenyl)acrylonitrile | HCID 10446442 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 4-[(Z)-2-cyano-2-(3,4-dimethoxy-phenyl)-vinyl]-phenyl acetate | HCID 10041861 | 95% |
Reaction Steps
Compound 1 (0.28 g) was acetylated with acetic anhydride and pyridine in accordance with a customary method, to thereby produce the target product (0.30 g, yield: 95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371773B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-788f0c6197a040d0a957ac8da95c5ae1 |
| Source note | uspto-grants-2008_05 |