HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dimethoxybenzeneacetonitrile → (z)-3-(3,5-Difluoro-phenyl)-2-(3,4-dimethoxy-phenyl)-acrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dimethoxybenzeneacetonitrile | HCID 66727 | — |
| Reactant | 3,5-Difluorobenzaldehyde | HCID 588160 | — |
| Product | (z)-3-(3,5-Difluoro-phenyl)-2-(3,4-dimethoxy-phenyl)-acrylonitrile | HCID 10424924 | 69.8% |
Reaction Steps
3,5-Difluorobenzaldehyde (1.42 g) and 3,4-dimethoxybenzyl cyanide (1.77 g) were subjected to condensation in accordance with process A of (production process 2), to thereby produce the target product (2.10 g, yield: 69%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371773B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-1a8ca7b1a846457aa6476bbe770bc95b |
| Source note | uspto-grants-2008_05 |