HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dimethoxybenzeneacetonitrile → (z)-2-(3,4-Dimethoxy-phenyl)-3-(2,4,5-trifluoro-phenyl)-acrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dimethoxybenzeneacetonitrile | HCID 66727 | — |
| Reactant | 2,4,5-Trifluorobenzaldehyde | HCID 519278 | — |
| Product | (z)-2-(3,4-Dimethoxy-phenyl)-3-(2,4,5-trifluoro-phenyl)-acrylonitrile | HCID 10358558 | 26% |
Reaction Steps
2,4,5-Trifluorobenzaldehyde (160 mg) and 3,4-dimethoxybenzyl cyanide (177 mg) were subjected to condensation in accordance with process B of (production process 2), to thereby produce the target product (80 mg, yield: 26%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371773B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-09b3a890437640488b984734f15f6497 |
| Source note | uspto-grants-2008_05 |