3-Nitrobenzaldehyde → HCID 9995520, compound

HRID 2222354Notes

Reaction equation

HRID 2222354 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][CH:11]=1)[CH:7]=O)([O-:3])=[O:2].[CH3:12][O:13][C:14]1[CH:15]=[C:16]([CH:20]=[CH:21][C:22]=1[O:23][CH3:24])[CH2:17][C:18]#[N:19]>>[CH3:12][O:13][C:14]1[CH:15]=[C:16](/[C:17](=[CH:7]/[C:6]2[CH:9]=[CH:10][CH:11]=[C:4]([N+:1]([O-:3])=[O:2])[CH:5]=2)/[C:18]#[N:19])[CH:20]=[CH:21][C:22]=1[O:23][CH3:24]

Participants

3

Reactant 2

HCID 74493-NitrobenzaldehydeHCID 667273,4-Dimethoxybenzeneacetonitrile

Product 1

HCID 9995520HCID 9995520, compoundYield 97%

Procedure

3-Nitrobenzaldehyde (3.02 g) and 3,4-dimethoxybenzyl cyanide (3.54 g) were subjected to condensation in accordance with process A of (production process 2), to thereby produce the target product (6.01 g, yield: 97%).

Sources & evidence

ORD record
ord-ea9a5ee2c50e4273a1d4fa0329cd3026
Source dataset
uspto-grants-2008_05
Patent number
US07371773B2

Reaction notes

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