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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2222355Generated: October 30, 2026

HCID 23089852, compound → HCID 10085056, compound

https://huagongshe.com/reaction/2222355

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 23089852HCID 23089852—
CatalystZincHCID 23994—
SolventAcetic AcidHCID 176—
ProductHCID 10085056HCID 1008505695.6%

Reaction Steps

Compound 19 (880 mg) was dissolved in acetic acid. Zinc powder was added to the resultant solution, and the resultant mixture was stirred for four hours. The mixture was concentrated to dryness under reduced pressure, followed by purification by use of a silica gel column, to thereby produce the target product (760 mg, yield: 95%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07371773B2
Source datasetuspto-grants-2008_05
ORD IDord-87fc718adf564676b6c4dc82edbbe678
Source noteuspto-grants-2008_05