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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2222372Generated: October 30, 2026

HCID 9995520, compound → HCID 9995865, compound

https://huagongshe.com/reaction/2222372

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 9995520HCID 9995520—
CatalystZincHCID 23994—
SolventAcetic AcidHCID 176—
ProductHCID 9995865HCID 999586580%

Reaction Steps

Compound 33 (1.80 g) was dissolved in acetic acid. Zinc powder was added to the resultant solution, and the resultant mixture was stirred for four hours. The mixture was concentrated to dryness under reduced pressure, followed by purification by use of a silica gel column, to thereby produce the target product (1.30 g, yield: 80%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07371773B2
Source datasetuspto-grants-2008_05
ORD IDord-7b6aef61cc9f49a1bfabc6aa7dc06924
Source noteuspto-grants-2008_05