HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9995520, compound → HCID 9995865, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9995520 | HCID 9995520 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 9995865 | HCID 9995865 | 80% |
Reaction Steps
Compound 33 (1.80 g) was dissolved in acetic acid. Zinc powder was added to the resultant solution, and the resultant mixture was stirred for four hours. The mixture was concentrated to dryness under reduced pressure, followed by purification by use of a silica gel column, to thereby produce the target product (1.30 g, yield: 80%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371773B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-7b6aef61cc9f49a1bfabc6aa7dc06924 |
| Source note | uspto-grants-2008_05 |