HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 68860790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Decanoic acid, 3-oxo-, ethyl ester | HCID 83224 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 68860790 | HCID 68860790 | — |
Reaction Steps
A solution of aniline (6 mmol), ethyl 3-oxodecanoate (6 mmol) and toluene-p-sulfonic acid (50 mg) in dry toluene (60 ml) was heated under reflux for 24 hours using Dean-Stark apparatus for the azeotropic removal of water. The solvent was removed in vacuum to afford the title product as an oil which was used without purification in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371779B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-76bd66c184634e898b72634b66da1508 |
| Source note | uspto-grants-2008_05 |