HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59712421, compound → HCID 23023483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59712421 | HCID 59712421 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23023483 | HCID 23023483 | 108.6% |
Reaction Steps
A solution of 0.409 g of methyl 2-[3-(t-butyldimethylsilanyloxymethyl)-4-ethoxybenzyl]tetrahydro-2-furancarboxylate in 20 ml of methanol was treated with 0.400 g of Dowex 50X ion-exchange resin for 6 hours, then the reaction mixture was filtrated and evaporated. The residue was purified by silica gel column chromatography, to give 0.320 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371777B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-55631405d0714ca8a046f508d60f1b47 |
| Source note | uspto-grants-2008_05 |