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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2222453Generated: November 1, 2026

HCID 59712421, compound → HCID 23023483, compound

https://huagongshe.com/reaction/2222453

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59712421HCID 59712421—
SolventMethanolHCID 887—
ProductHCID 23023483HCID 23023483108.6%

Reaction Steps

A solution of 0.409 g of methyl 2-[3-(t-butyldimethylsilanyloxymethyl)-4-ethoxybenzyl]tetrahydro-2-furancarboxylate in 20 ml of methanol was treated with 0.400 g of Dowex 50X ion-exchange resin for 6 hours, then the reaction mixture was filtrated and evaporated. The residue was purified by silica gel column chromatography, to give 0.320 g of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07371777B2
Source datasetuspto-grants-2008_05
ORD IDord-55631405d0714ca8a046f508d60f1b47
Source noteuspto-grants-2008_05