Hydrochloric Acid → HCID 17856383, compound

Participants

Reaction Steps

The 1-[(o-chlorophenyl)iminomethyl]cyclopentanol hydrochloride 3 was prepared by dissolving 20 g (0.089 mol) of the free base of compound 3 in 25 ml of isopropanol and to this solution was added 100 ml of hydrochloric acid (2N) in diethyl ether. The mixture was then stirred for 10 minutes, and the precipitate obtained was filtered, washed by diethyl ether and dried to give a white solid of the hydrochloride of compound 3 (23.14 g, 100%).

Provenance & Evidence