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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2222568Generated: November 2, 2026

Phthalimide potassium salt → HCID 69101686, compound

https://huagongshe.com/reaction/2222568

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhthalimide potassium saltHCID 24194345—
ReactantHCID 91605735HCID 91605735—
SolventAcetoneHCID 180—
ProductHCID 69101686HCID 69101686—

Reaction Steps

The 1,10-Diiodo-dec-5-ene (1 equiv.) is dissolved in anhydrous acetone at ambient temperature followed by the addition of potassium phthalimide (4. equiv.). The reaction mixture is stirred until completion, washed with brine, dried over magnesium sulfate, and concentrated in vacuo. The crude product is purified via silica gel chromatography to afford 1,10-dipthalimido-dec-5-ene.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07371852B2
Source datasetuspto-grants-2008_05
ORD IDord-863940e65bda474db777218e1e18dfc2
Source noteuspto-grants-2008_05