HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalimide potassium salt → HCID 69101686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Reactant | HCID 91605735 | HCID 91605735 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 69101686 | HCID 69101686 | — |
Reaction Steps
The 1,10-Diiodo-dec-5-ene (1 equiv.) is dissolved in anhydrous acetone at ambient temperature followed by the addition of potassium phthalimide (4. equiv.). The reaction mixture is stirred until completion, washed with brine, dried over magnesium sulfate, and concentrated in vacuo. The crude product is purified via silica gel chromatography to afford 1,10-dipthalimido-dec-5-ene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371852B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-863940e65bda474db777218e1e18dfc2 |
| Source note | uspto-grants-2008_05 |