Hydrazine → HCID 86594829, compound

HRID 2222569Notes

Reaction equation

HRID 2222569 reaction equation
C1(=O)[N:5]([CH2:6][CH2:7][CH2:8][CH2:9][CH:10]=[CH:11][CH2:12][CH2:13][CH2:14][CH2:15][N:16]2C(=O)C3=CC=CC=C3C2=O)C(=O)C2=CC=CC=C12.NN>C(O)C>[NH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH:10]=[CH:11][CH2:12][CH2:13][CH2:14][CH2:15][NH2:16]

Participants

4

Reactant 2

HCID 9321HydrazineHCID 69101686HCID 69101686, compound

Product 1

HCID 86594829HCID 86594829, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The 1,10-dipthalimido-dec-5-ene (1 equiv.) and hydrazine (2 equiv.) are stirred in ethanol at reflux. The reaction mixture is cooled to room temperature and the resulting solid is filtered off. The filtrate is purified via silica gel chromatography to yield 1,10 diamino-dec-5-ene.

Workup

  1. temperatureat reflux
  2. filtrationthe resulting solid is filtered off
  3. customThe filtrate is purified via silica gel chromatography

Sources & evidence

ORD record
ord-fd822b020566406e81280c960f622e52
Source dataset
uspto-grants-2008_05
Patent number
US07371852B2

Reaction notes

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