HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 86594829, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 69101686 | HCID 69101686 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86594829 | HCID 86594829 | — |
Reaction Steps
The 1,10-dipthalimido-dec-5-ene (1 equiv.) and hydrazine (2 equiv.) are stirred in ethanol at reflux. The reaction mixture is cooled to room temperature and the resulting solid is filtered off. The filtrate is purified via silica gel chromatography to yield 1,10 diamino-dec-5-ene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371852B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-fd822b020566406e81280c960f622e52 |
| Source note | uspto-grants-2008_05 |