HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 69101980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 69101410 | HCID 69101410 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69101980 | HCID 69101980 | — |
Reaction Steps
1,10-diphthalimido-1-pyridinyldecane (1 equiv.) and hydrazine (2 equiv.) are stirred in ethanol at reflux. The reaction mixture is cooled to room temperature and the resulting solid is filtered off. The filtrate is purified by silica gel chromatography to yield 1,10-diamino-1-pyridinyldecane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371852B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-b06b8678bd64441a89d451595236f788 |
| Source note | uspto-grants-2008_05 |