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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2222572Generated: October 30, 2026

Hydrazine → HCID 69101980, compound

https://huagongshe.com/reaction/2222572

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazineHCID 9321—
ReactantHCID 69101410HCID 69101410—
SolventEthanolHCID 702—
ProductHCID 69101980HCID 69101980—

Reaction Steps

1,10-diphthalimido-1-pyridinyldecane (1 equiv.) and hydrazine (2 equiv.) are stirred in ethanol at reflux. The reaction mixture is cooled to room temperature and the resulting solid is filtered off. The filtrate is purified by silica gel chromatography to yield 1,10-diamino-1-pyridinyldecane.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07371852B2
Source datasetuspto-grants-2008_05
ORD IDord-b06b8678bd64441a89d451595236f788
Source noteuspto-grants-2008_05