HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 58664769, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Hydroxybenzotriazole | HCID 75771 | — |
| Reactant | 2-Aminoimidazole | HCID 82140 | — |
| Reactant | O-(Benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate | HCID 2733207 | — |
| Reactant | HCID 58664765 | HCID 58664765 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 58664769 | HCID 58664769 | — |
Reaction Steps
3.2 g of 14 are reacted with 1.88 g of 2-aminoimidazole, 2.96 g of TBTU, 0.29 g of HOBt and 2.95 g of potassium carbonate in 40 ml of DMF analogously to the preparation of 5. Conventional work-up gives 15.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371854B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-06277a23137843038eb5c2475cf6c477 |
| Source note | uspto-grants-2008_05 |