HRID2223703

反应详情

EQUATION

反应方程式

HRID 2223703 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 4-(2-methoxy-phenyl)-3,6-dihydro-2H-pyridine-1-carboxylic acid tert-butyl ester (200 mg, 0.69 mmol), Pd—C 10% (30 mg) in EtOAc (5 mL) is hydrogenated at room temperature and atmospheric pressure for 20 h. The mixture is filtered over Celite, and the filtrate is evaporated to provide the title compound.

WORKUP

后处理

  1. customis hydrogenated at room temperature
  2. filtrationThe mixture is filtered over Celite
  3. customthe filtrate is evaporated