Acetic Anhydride → HCID 23021166, compound

Participants

Reaction Steps

To 3-[1-(triethylsiloxymethyl)cyclohexyl]propan-1-ol (410 mg) were added acetic anhydride (3 mL) and pyridine (3 mL) at room temperature. The solution was stirred at room temperature for 2 hours and concentrated under reduced pressure. The residue was distilled with toluene azeotropically to give the title compound (480 mg). This product was subjected to the subsequent step without further pirification.

Provenance & Evidence