HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 59714905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 59714981 | HCID 59714981 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 59714905 | HCID 59714905 | — |
Reaction Steps
To a solution of 2-[2-[1-[2-(tert-butyldiphenylsiloxy)ethyl]cyclohexyl]ethyl]-2-hydroxymethylbutan-1,4-diol (300 mg) in pyridine (5.0 mL) was added acetic anhydride (5.0 mL) at room temperature. After stirring the solution at room temperature for 16 hours, it was concentrated under reduced pressure to give the title compound (340 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07375115B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-e70ef739c7ab48bf983e4c33855f8c5a |
| Source note | uspto-grants-2008_05 |