HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59714980, compound → HCID 59714922, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59714980 | HCID 59714980 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 59714922 | HCID 59714922 | 129.9% |
Reaction Steps
tert-Butyl [2-[1-[2-[4-[N-(5-methylpyridin-2-yl)-2-furancarboxamido]piperidin-1-yl]ethyl]cyclohexyl]ethyl]carbamate (0.4760 g) was dissolved in a 4N hydrochloric acid/1,4-dioxane solution (10.0 mL) and methanol (5 mL). The solution was stirred at room temperature for 2 hours. The solvent was distilled off under reduced pressure to give the title compound (0.5036 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07375115B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-a2d74cdea1b54d78acb3038bc279c670 |
| Source note | uspto-grants-2008_05 |