HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Chloropyridin-3-yl)methanol → 3-(Bromomethyl)-2-chloropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Chloropyridin-3-yl)methanol | HCID 2763647 | — |
| Reactant | 3-(Bromomethyl)-2,6-dichloro-5-fluoropyridine | HCID 59717573 | — |
| Product | 3-(Bromomethyl)-2-chloropyridine | HCID 18931028 | 78% |
Reaction Steps
Compound 12B (0.22 g, 78%) was prepared from 12A (0.20 g, 1.39 mmol) using a procedure similar to the synthesis of 1B. HPLC Rt=1.94 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-14a4f5c969c4475ebf6f1875d117b296 |
| Source note | uspto-grants-2008_05 |