HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichloronicotinic acid → (2,6-Dichloropyridin-3-yl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichloronicotinic acid | HCID 854047 | — |
| Reactant | (2,6-Dichloro-5-fluoropyridin-3-yl)methanol | HCID 23114857 | — |
| Product | (2,6-Dichloropyridin-3-yl)methanol | HCID 12259932 | 89% |
Reaction Steps
Compound 13A (0.82 g, 89%) was prepared from 2,6-dichloro-nicotinic acid (1.0 g, 5.2 mmol) using a procedure similar to the synthesis of 1A. HPLC Rt=1.39 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-5a582b314f9a43f8b9766d6dca217e8e |
| Source note | uspto-grants-2008_05 |