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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2224319Generated: October 30, 2026

3-(Bromomethyl)-2,6-dichloropyridine → 6-Acetyl-2-chloro-5,6-dihydropyrido[3,2-c][1]benzazocine

https://huagongshe.com/reaction/2224319

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-(Bromomethyl)-2,6-dichloropyridineHCID 12265394—
Reactant6-Acetyl-2-chloro-3-fluoro-5,6-dihydro-pyrido[3,2-c][1]benzazocineHCID 74393412—
Product6-Acetyl-2-chloro-5,6-dihydropyrido[3,2-c][1]benzazocineHCID 72820179—

Reaction Steps

Compound 13C was prepared from bb and 13B by a route analogous to that used for the preparation of 1D. HPLC Rt=2.493 min; LCMS Found: (M+H)+=285.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07378426B2
Source datasetuspto-grants-2008_05
ORD IDord-2019b49b2cda4e10ac154d57f8a64515
Source noteuspto-grants-2008_05