HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 69289265, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | 6-Acetyl-3-fluoro-5,6-dihydro-2-(6-methoxy-3-pyridinyl)-pyrido[3,2-c][1]benzazocine | HCID 69291197 | — |
| Product | HCID 69289265 | HCID 69289265 | 87% |
Reaction Steps
The title compound (19.9 mg, 87%) was prepared from 13C (20.0 mg, 0.07 mmol) and phenylboronic acid (12.8 mg, 0.105 mmol) by a route analogous to that used for the preparation of 2B. HPLC Rt=2.353 min; LCMS Found: (M+H)+=327.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-834d9c17a9734d5a8695cdd8a2268ea2 |
| Source note | uspto-grants-2008_05 |