HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Iodo-4-pyridinemethanol → 6-Acetyl-5,6-dihydropyrido[4,3-c][1]benzazocine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Iodo-4-pyridinemethanol | HCID 23106621 | — |
| Reactant | 6-Acetyl-2-chloro-3-fluoro-5,6-dihydro-pyrido[3,2-c][1]benzazocine | HCID 74393412 | — |
| Product | 6-Acetyl-5,6-dihydropyrido[4,3-c][1]benzazocine | HCID 69289286 | — |
Reaction Steps
Compound 24C was prepared from 24A and bb in two steps by a route analogous to that used for the preparation of 1D. HPLC Rt=1.383 min; LCMS Found: (M+H)+=251.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-2c90e016997b4176b7272849474422c7 |
| Source note | uspto-grants-2008_05 |