HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Chloro-5-iodo-pyridin-4-yl)-methanol → 4-Bromomethyl-2-chloro-5-iodo-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Chloro-5-iodo-pyridin-4-yl)-methanol | HCID 59717559 | — |
| Reactant | 3-(Bromomethyl)-2,6-dichloro-5-fluoropyridine | HCID 59717573 | — |
| Product | 4-Bromomethyl-2-chloro-5-iodo-pyridine | HCID 59717563 | 60% |
Reaction Steps
Compound 25D (0.28 g, 60%) was prepared from 25C (0.38 g, 1.4 mmol) using a procedure similar to the synthesis of 1B. HPLC Rt=2.72 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-e4f22f5af1d14b2c9dfb3d19fe25a480 |
| Source note | uspto-grants-2008_05 |