HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromomethyl-2-chloro-5-iodo-pyridine → 6-Acetyl-3-chloro-5,6-dihydropyrido[4,3-c][1]benzazocine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromomethyl-2-chloro-5-iodo-pyridine | HCID 59717563 | — |
| Reactant | 6-Acetyl-2-chloro-3-fluoro-5,6-dihydro-pyrido[3,2-c][1]benzazocine | HCID 74393412 | — |
| Product | 6-Acetyl-3-chloro-5,6-dihydropyrido[4,3-c][1]benzazocine | HCID 72366783 | — |
Reaction Steps
Compound 25E was prepared from 25D and bb in two steps by a route analogous to that used for the preparation of 1D. HPLC Rt=2.506 min; LCMS Found: (M+H)+=285.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-edd44406225d4ae680054aa315dbe60b |
| Source note | uspto-grants-2008_05 |