HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Acetylphenylboronic acid → HCID 69292962, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Acetylphenylboronic acid | HCID 2734309 | — |
| Reactant | 6-Acetyl-3-fluoro-5,6-dihydro-2-(6-methoxy-3-pyridinyl)-pyrido[3,2-c][1]benzazocine | HCID 69291197 | — |
| Reactant | 6-Acetyl-3-chloro-5,6-dihydropyrido[4,3-c][1]benzazocine | HCID 72366783 | — |
| Product | HCID 69292962 | HCID 69292962 | 70% |
Reaction Steps
The title compound (12.0 mg, 70%) was prepared from 25E (16.0 mg, 0.055 mmol) and 2-acetylphenylboronic acid (13.8 mg, 0.079 mmol) by a route analogous to that used for the preparation of 2B. HPLC Rt=2.05 min; LCMS Found: (M+H)+=367.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-a32db028f5964bb38916862d72556325 |
| Source note | uspto-grants-2008_05 |