HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromomethyl-2-chloro-5-iodo-pyridine → 6-Acetyl-3,9-dichloro-5,6-dihydropyrido[4,3-c][1]benzazocine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromomethyl-2-chloro-5-iodo-pyridine | HCID 59717563 | — |
| Reactant | N-(4-chloro-2-vinyl-phenyl)-acetamide | HCID 59717611 | — |
| Reactant | 6-Acetyl-2-chloro-3-fluoro-5,6-dihydro-pyrido[3,2-c][1]benzazocine | HCID 74393412 | — |
| Product | 6-Acetyl-3,9-dichloro-5,6-dihydropyrido[4,3-c][1]benzazocine | HCID 72366780 | — |
Reaction Steps
The title compound was prepared from 25D and 9B in two steps by a route analogous to that used for the preparation of 1D. HPLC Rt=2.836 min; LCMS Found: (M+H)+=319.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-dd9c3585fc1846f7b798fe1dff217283 |
| Source note | uspto-grants-2008_05 |