HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,6-Dichloronicotinic acid → (4,6-Dichloropyridin-3-yl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,6-Dichloronicotinic acid | HCID 817158 | — |
| Reactant | (2,6-Dichloro-5-fluoropyridin-3-yl)methanol | HCID 23114857 | — |
| Product | (4,6-Dichloropyridin-3-yl)methanol | HCID 2762727 | 60% |
Reaction Steps
Compound 41A (2.5 g, 60%) was prepared from 4,6-dichloro-nicotinic acid (4.5 g, 23.4 mmol) using a procedure similar to the synthesis of 1A.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-366862b48ec549de8844653d1791a9bd |
| Source note | uspto-grants-2008_05 |