HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Iodopicolinic acid → (3-Iodopyridin-2-yl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Iodopicolinic acid | HCID 11253692 | — |
| Reactant | (2,6-Dichloro-5-fluoropyridin-3-yl)methanol | HCID 23114857 | — |
| Product | (3-Iodopyridin-2-yl)methanol | HCID 59717577 | 10.6% |
Reaction Steps
Compound 51A (10 mg, 10%) was prepared from 3-iodo-pyridine-2-carboxylic acid (100 mg, 0.4 mmol) ) using a procedure similar to the synthesis of 1A. HPLC Rt=0.3 min
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-d37374855e164e74b6f18014674ccef6 |
| Source note | uspto-grants-2008_05 |