HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3-iodo-pyridin-2-ylmethyl)-N-(2-vinyl-phenyl)-acetamide → 11-Acetyl-11,12-dihydropyrido[2,3-c][1]benzazocine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3-iodo-pyridin-2-ylmethyl)-N-(2-vinyl-phenyl)-acetamide | HCID 59717574 | — |
| Reactant | 6-Acetyl-2-chloro-3-fluoro-5,6-dihydro-pyrido[3,2-c][1]benzazocine | HCID 74393412 | — |
| Product | 11-Acetyl-11,12-dihydropyrido[2,3-c][1]benzazocine | HCID 69291019 | 55% |
Reaction Steps
Compound 51D (3.1 mg, 55%) was prepared from 51C (8.5 mg, 0.0225 mmol) by a route analogous to that used for the preparation of 1D. HPLC Rt=1.503 min; LCMS Found: (M+H)+=251.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-50a68d039b4049aba98c4fedadcb2224 |
| Source note | uspto-grants-2008_05 |