HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine → HCID 69291047, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine | HCID 16217714 | — |
| Reactant | 1-(3-bromo-12H-1,11-diaza-dibenzo[a,e]cycloocten-11-yl)-ethanone | HCID 69289275 | — |
| Reactant | 6-Acetyl-3-fluoro-5,6-dihydro-2-(6-methoxy-3-pyridinyl)-pyrido[3,2-c][1]benzazocine | HCID 69291197 | — |
| Product | HCID 69291047 | HCID 69291047 | 95.9% |
Reaction Steps
Compound 52D (20.9 mg, 91%) was prepared from 52C (20 mg, 0.061 mmol) and 2A (14.3 mg, 0.061 mmol) by a route analogous to that used for the preparation of 2B. HPLC Rt=2.419 min; LCMS Found: (M+H)+=358.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-4c79482fb0c84cdeb2e3151701f7f6af |
| Source note | uspto-grants-2008_05 |