HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-6-chloro-2-methylpyridine → 3-Bromo-2-(bromomethyl)-6-chloropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-6-chloro-2-methylpyridine | HCID 14866674 | — |
| Reactant | 3,5-Dibromo-2-(bromomethyl)pyridine | HCID 53417177 | — |
| Product | 3-Bromo-2-(bromomethyl)-6-chloropyridine | HCID 23249915 | 45% |
Reaction Steps
Compound 55B (0.33 g, 45%) was prepared from 55A (0.53 g, 2.57 mmol) using a procedure similar to the synthesis of 52B. HPLC Rt=2.47 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-e81759140f404bed8febb149f307e60d |
| Source note | uspto-grants-2008_05 |