HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 69292204, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | 6-Acetyl-3-fluoro-5,6-dihydro-2-(6-methoxy-3-pyridinyl)-pyrido[3,2-c][1]benzazocine | HCID 69291197 | — |
| Reactant | 1-(2-chloro-12H-1,11-diaza-dibenzo[a,e]cycloocten-11-yl)-ethanone | HCID 72366779 | — |
| Product | HCID 69292204 | HCID 69292204 | 102.1% |
Reaction Steps
Compound 55D (6.0 mg, 100%) was prepared from 55C (5.0 mg, 0.018 mmol) and phenylboronic acid (2.2 mg, 0.018 mmol) by a route analogous to that used for the preparation of 2B. HPLC Rt=2.729 min; LCMS Found: (M+H)+=327.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-6653363787fd419f82744ca3a74752c5 |
| Source note | uspto-grants-2008_05 |