HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Dihydroxyboranyl)benzoic acid → 2-(11-Acetyl-11,12-dihydro-1,11-diaza-dibenzo[a,e]cycloocten-2-yl)-benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Dihydroxyboranyl)benzoic acid | HCID 2733985 | — |
| Reactant | 6-Acetyl-3-fluoro-5,6-dihydro-2-(6-methoxy-3-pyridinyl)-pyrido[3,2-c][1]benzazocine | HCID 69291197 | — |
| Reactant | 1-(2-chloro-12H-1,11-diaza-dibenzo[a,e]cycloocten-11-yl)-ethanone | HCID 72366779 | — |
| Product | 2-(11-Acetyl-11,12-dihydro-1,11-diaza-dibenzo[a,e]cycloocten-2-yl)-benzoic acid | HCID 69291538 | — |
Reaction Steps
Compound 61A was prepared from 55C (17 mg, 0.060 mmol) and 2-carboxyphenylboronic acid (10 mg, 0.060 mmol) by a route analogous to that used for the preparation of 2B.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-950306c94ce2466ca2bbcec98cd16ecd |
| Source note | uspto-grants-2008_05 |