HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-5-(chloromethyl)pyrimidine → HCID 72366781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-5-(chloromethyl)pyrimidine | HCID 13568279 | — |
| Reactant | 6-Acetyl-2-chloro-3-fluoro-5,6-dihydro-pyrido[3,2-c][1]benzazocine | HCID 74393412 | — |
| Product | HCID 72366781 | HCID 72366781 | 46% |
Reaction Steps
Compound 64B (66.1 mg, 46%) was prepared from 64A (0.10 g, 0.5 mmol) and bb (82 mg, 0.5 mmol) in two steps by a route analogous to that used for the preparation of 1D. HPLC Rt=2.286 min; LCMS Found: (M+H)+=286.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-6e9609623108426998d50dc99277f512 |
| Source note | uspto-grants-2008_05 |