HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol, 2-[(3-aminophenyl)sulfonyl]- → HCID 11541170, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol, 2-[(3-aminophenyl)sulfonyl]- | HCID 78905 | — |
| Reactant | (3-Nitrophenyl)methanesulfonyl chloride | HCID 13196775 | — |
| Reactant | 7-Trifluoromethyl-5-(4-trifluoromethyl-phenyl)-pyrazolo[1,5-a]pyrimidine-3-carboxylic acid | HCID 86607112 | — |
| Product | HCID 11541170 | HCID 11541170 | — |
Reaction Steps
The title compound was prepared from 7-trifluoromethyl-5-(4-trifluoromethyl-phenyl)-pyrazolo[1,5-a]pyrimidine-3-carboxylic acid (example C.2) and 3-(2-hydroxy-ethanesulfonyl)-aniline [CAS-Nr. 344750-15-8; prepared from commercially available 3-nitro-phenylmethane-sulfonyl chloride] according to general procedure II. Yellow solid. MS (ISP) 542.0 [(M−H)−]; mp 298° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378417B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-eeb87425cf414d79bdcca672c6744528 |
| Source note | uspto-grants-2008_05 |