Sodium Methoxide → HCID 11561583, compound

Participants

Reaction Steps

The title compound was prepared by stirring 7-chloro-5-(4-chloro-phenyl)-pyrazolo[1,5-a]pyrimidine-3-carboxylic acid(3-methanesulfonyl-phenyl)-amide (example 175) (46 mg) with a solution of sodium methoxide (11 mg) in methanol (1.5 mL) for 2 h at 50° C., followed by precipitation of the product by the addition of water (10 mL). Pale-yellow solid. MS (ISP) 457.5 [(M+H)+]; mp 265° C.

Provenance & Evidence