HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68870329, compound → HCID 68871351, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68870329 | HCID 68870329 | — |
| Reactant | HCID 68871587 | HCID 68871587 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68871351 | HCID 68871351 | — |
Reaction Steps
The title compound was prepared according to the procedure of Example 22E, substituting the product of Example 23A, for the product of Example 22D. 1H NMR (300 MHz, CDCl3): δ 0.88 (m, 7 H) 1.06 (m, 1 H) 1.48 (m, 1 H) 1.55 (s, 3 H) 1.96 (m, 2 H) 3.76 (m, 2 H) 5.03 (m, 1 H) 5.83 (d, J=6.99 Hz, 1 H) 7.06 (m, 4 H) 7.29 (m, 5 H). Specific rotation: [α]D +12.4° (c 2.16, EtOH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378414B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-cd93b28d57b04b2c9246f31d163cfa9d |
| Source note | uspto-grants-2008_05 |