Sodium Hydroxide → HCID 68873989, compound

Participants

Reaction Conditions

Reaction Steps

A suspension of the product of Example 36I (0.77 g) in water (2 mL) was treated with 0.997N sodium hydroxide solution (0.161 mL, 0.160 mmol) and stirred at 25° C. for 1 hour. The solution was lyophilized to give the title compound (0.79 g, 99%). 1H NMR (300 MHz, DMSO-d6): δ ppm 0.84 m, 11 H) 1.45 m, 7 H) 1.68 m, 1 H) 2.10 m, 1 H) 7.31 m, 3 H) 7.49 m, 3 H) 7.65 m, 1 H) 8.05 m, 1 H) 15.45 m, 1 H). MS (ESI−) m/z 477 (M−H)−.

Provenance & Evidence