HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 11235514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 10222876 | HCID 10222876 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 11235514 | HCID 11235514 | 90% |
Reaction Steps
Compound 1 (170 mg, 0.4 mmle) in 10 mL THF was treated with NH3 at 25° C. After 30 mins, the precipitate formed in the reaction was filtered out to give Compound 17 in a yield of 90%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378532B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-ec8ea9d276a146b28de6c1c57951643a |
| Source note | uspto-grants-2008_05 |