Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 58393283 | HCID 58393283 | — |
| Solvent | Toluene | HCID 1140 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 59449243 | HCID 59449243 | — |
Reaction Steps
8.57 ml (8.57 mmol) of a 1 M solution of lithium aluminium hydride in toluene were dissolved in 8 ml THF and at ambient temperature slowly combined with 850 mg (2.86 mmol) of product from Example 4 (J) dissolved in 2 ml THF. The reaction solution was stirred for 2 hours at 75° C. Then 1N sodium hydroxide solution and water were added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08207335B2 |
|---|
| Source dataset | uspto-grants-2012_06 |
|---|
| ORD ID | ord-a49e6f98a0c94124b717b718c9d9f968 |
|---|
| Source note | uspto-grants-2012_06 |
|---|
