HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylpiperidine → 1-(4-Acetoxy-3-methoxycinnamoyl)-4-methylpiperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylpiperidine | HCID 69381 | — |
| Reactant | 4-Acetoxy-3-methoxycinnamoyl chloride | HCID 54468022 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 1-(4-Acetoxy-3-methoxycinnamoyl)-4-methylpiperidine | HCID 54136428 | — |
Reaction Steps
Using 5.09 g of 4-acetoxy-3-methoxycinnamoyl chloride, 2.4 ml of 4-methylpiperidine, and 100 ml of pyridine, a reaction similar to that conducted in Example 53 was carried out. As a result, 5.2 g of 1-(4-acetoxy-3-methoxycinnamoyl)-4-methylpiperidine (a compound of the present invention) was obtained as an orange-yellow oil, which had the following physiochemical properties:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344845 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-9b3a5e860ace429da7458b6edcfc51f4 |
| Source note | uspto-grants-1994_09 |