HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → N-cyclohexyl-4-hydroxy-3-methoxycinnamamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-cyclohexyl-4-acetoxy-3-methoxycinnamamide | HCID 54552956 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-cyclohexyl-4-hydroxy-3-methoxycinnamamide | HCID 54188453 | 101.3% |
Reaction Steps
Using 2.64 g of N-cyclohexyl-4-acetoxy-3-methoxycinnamamide (Example 57), 70 ml of methanol, and 5 g of potassium carbonate, a reaction similar to that conducted in Example 54 was carried out. As a result, 2.32 g of N-cyclohexyl-4-hydroxy-3-methoxycinnamamide (a compound of the present invention) was obtained as white crystal, which had the following physiochemical properties:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344845 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-244ac2bbda19482ab19c178ce3ac3724 |
| Source note | uspto-grants-1994_09 |