Diethyl chlorophosphate → HCID 178483958, compound

Participants

Reaction Steps

Using 6.5 ml of diethyl chlorophosphate, 18 ml of triethylamine, 5.2 g of dimethylaminoglycine hydrochloride, 5 g of cis-4-methylcyclohexylammonium chloride, and 0.15 g of 4-dimethylaminopyridine, a reaction similar to that performed in Example 77 was carried out. As a result, 4.8 g of N-(cis-4-methylcyclohexyl)-2-dimethylaminoacetamide was obtained as a pale yellow oil, which had the following physiochemical properties:

Provenance & Evidence