HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4'-Bipiperidine → HCID 178490539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4'-Bipiperidine | HCID 78607 | — |
| Reactant | 3-(3-Methoxyphenyl)prop-2-enamide | HCID 57296506 | — |
| Solvent | Methyl Isobutyl Ketone | HCID 7909 | — |
| Product | HCID 178490539 | HCID 178490539 | — |
Reaction Steps
Using 1.9 g N-(trans-4-methylcyclohexyl)-4-chloroethoxy)-3-methoxycinnamamide (Example 138), 4.56 g of 4-piperidinopiperidine, and 50 ml of methylisobutylketone, a reaction similar to that conducted in Example 142 was carried out. As a result, 1.51 g of N-(trans-4-methylcyclohexyl)-4-[2-(4-piperidinopiperidino)ethoxy]-3-methoxycinnamamide (a compound of the present invention) was obtained as white crystal, which had the following physiochemical properties:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344845 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-c577ee254a294632aaeab912c4601104 |
| Source note | uspto-grants-1994_09 |