HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178462640, compound → HCID 178462641, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178462640 | HCID 178462640 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178462641 | HCID 178462641 | 69.7% |
Reaction Steps
Using 0.2 g of N-(trans-4-methylcyclohexyl)-4-{2-[1-(2-ethyl)imidazoly]ethoxy}-3-methoxycinnamamide (Example 162), 0.01 g of 10% palladium-carbon, and 25 ml of methanol, a reaction similar to that conducted in Example 147 was performed. As a result, 0.14 g of N-(trans-4-methylcyclohexyl)-3-{4-{2-[1-(2-ethyl)imidazolyl]ethoxy}-3-methoxyphenyl}propionamide (a compound of the present invention) was obtained as white crystal, which had the following physiochemical properties:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344845 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-aa3bc92f69f64f518bbc3595fae6109e |
| Source note | uspto-grants-1994_09 |