HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178490527, compound → HCID 178490528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178490527 | HCID 178490527 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178490528 | HCID 178490528 | 64.7% |
Reaction Steps
Using 0.2 g of N-(trans-4-methylcyclohexyl)-4-(3-carboxypropoxy) -3-methoxycinnamamide (Example 175), 0.01 g of 10% palladium-carbon, and 35 ml of methanol, a reaction similar to that conducted in Example 147 was carried out. As a result, 0.13 g of N-(trans-4-methylcyclohexyl) -3-[4-(3-carboxypropoxy)-3-methoxyphenyl]propionamide (a compound of the present invention) was obtained as white crystal, which had the following physiochemical properties:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344845 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-dc5fd6df73c143a884b4341e2f55f570 |
| Source note | uspto-grants-1994_09 |