HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178490517, compound → HCID 178490518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178490517 | HCID 178490517 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178490518 | HCID 178490518 | 49.7% |
Reaction Steps
Using 0.1 g of N-(trans-4-methylcyclohexyl )-4-(2-pyrazolylethoxy) -3-methoxycinnamamide (Example 180), 0.007 g of 10% palladium-carbon, and 30 ml of methanol, a reaction similar to that conducted in Example 147 was carried out. As a result, 0.05 g of N-(trans-4-methylcyclohexyl) -3-[4-(2-pyrazolylethoxy)-3methoxyphenyl]propionamide (a compound of the present invention) was obtained as light-yellowish brown crystal, which had the following physiochemical properties:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344845 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-43d22f83409e4a3e9cb02379b9386992 |
| Source note | uspto-grants-1994_09 |