HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl phenylglyoxalate → HCID 19004392, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl phenylglyoxalate | HCID 84835 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 19004392 | HCID 19004392 | 112.4% |
Reaction Steps
A mixture of 4-[(2-phenylethyl)oxy)]-alpha-oxobenzeneacetic acid methyl ester (0.4 g) in methanol and 0.5N sodium hydroxide (8 mL) was treated as in Example 19 and the crude product was crystallized from benzene-hexane to give 0.37 g of 4-[(2-phenylethyl)oxy]-alpha-oxobenzeneacetic acid as a colorless solid, mp 72°-73° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344843 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-4d1e675db3c14f3d9b9b0ef75732be82 |
| Source note | uspto-grants-1994_09 |